The process of measuring titratable acidity (TA) involves a few key steps. Here’s a simplified outline of how it’s typically done:
Materials Needed:
– Sample Solution (e.g., wine, juice, milk, coffee)
– Strong Base (e.g., sodium hydroxide, NaOH)
– pH Indicator (e.g., phenolphthalein)
– Burette
– Erlenmeyer Flask or Beaker
– Stirring Rod or Magnetic Stirrer
– pH Meter (optional)
Steps to Measure Titratable Acidity:
1. Prepare the Sample:
– Accurately measure a known volume of the sample solution and place it in an Erlenmeyer flask or beaker.
2. Add the pH Indicator:
– Add a few drops of a pH indicator to the sample. Phenolphthalein is commonly used because it changes color at around pH 8.2 to 9.8.
3. Titrate with Base:
– Fill a burette with a standardized strong base solution (e.g., 0.1 N NaOH).
– Slowly add the base to the sample solution while continuously stirring. A magnetic stirrer can help ensure thorough mixing.
– Carefully observe the color change in the sample solution. If using a pH meter, titrate until the desired endpoint pH is reached (commonly around pH 8.2 or 8.4 for phenolphthalein).
4. Record the Volume:
– Note the volume of base solution used to reach the endpoint. This is where the color changes or the pH meter reads the target pH.
5. Calculate Titratable Acidity:
– Use the volume of the base solution added to calculate the TA. Use the concentration of the base too. Also, consider the known volume of the sample. The formula is usually:

The result is typically expressed in terms of a specific acid. This can be in grams per liter (g/L) or milligrams per 100 milliliters (mg/100mL). The choice depends on the context and standard practices for the sample being tested.
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